乙酰丙酮分光光度法测定建筑防火涂料中的甲醛含量-绿色装修网.PDF

第 卷 年第 期 Q 质量检测 30 2012 4 uality Test 乙酰丙酮分光光度法 测定建筑防火涂料中的甲醛含量 1 1 2 2 张 丹 路艳罗 龚万森 王志霞 1. 100029 2. 100013 （北京化工大学化工资源有效利用国家重点实验室，北京 ；国家建筑工程质量监督检验中心，北京 ） 【摘要】 参照GB 18582-2008 标准，采用乙酰丙酮作显色剂，分光光度法对建筑防火涂料中的游离甲醛含量进行了检测。 0 ~ 80 g 0.9997 20 g ~ 80 g 92.73% ～ 99.55% 测定甲醛的线性范围为 μ ，相关系数为 ， μ μ 甲醛含量的加标回收率为 ，相对标准偏 差小于1.5%。该方法简便快速，灵敏度高，适于建筑防火涂料中甲醛的测定。 【关键词】 分光光度法；乙酰丙酮；建筑防火涂料；甲醛 【中图分类号】 TU54 【文献标识码】 A 【文章编号】 1671 3702 2012 04 04 － （ ） －0007－ Determination of Formaldehyde in Building Fire-Retardant Coatings by Acetylacetone Spectrophotometry ZHANG Dan1 LU Yan-luo1 GONG Wan-sen2 WANG Zhi-xia2 (1.State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing 100029, China; 2.National center for quality supervision and test of building engineering, Beijing 100013, China) Abstract: This paper described the measurement of the concentration of formaldehyde in building Fire-Retardant coatings with acetylacetone spectrophotometry according to the standard of GB 18582-2008.The linear range of formaldehyde was 0 ～80μg, the correlative was 0.9997, the recovery was 92.73%～99.55% and RSD was less than 1.5%. The method was simple, rapid, sensitive and proved to be suitable for determination of free formaldehyde in building fire-retardant coatings. Keywords: spectrophotometry; ace