原创力文档- 1、原创力文档（book118）网站文档一经付费（服务费），不意味着购买了该文档的版权，仅供个人/单位学习、研究之用，不得用于商业用途，未经授权，严禁复制、发行、汇编、翻译或者网络传播等，侵权必究。。
- 2、本站所有内容均由合作方或网友上传，本站不对文档的完整性、权威性及其观点立场正确性做任何保证或承诺！文档内容仅供研究参考，付费前请自行鉴别。如您付费，意味着您自己接受本站规则且自行承担风险，本站不退款、不进行额外附加服务；查看《如何避免下载的几个坑》。如果您已付费下载过本站文档，您可以点击 这里二次下载。
- 3、如文档侵犯商业秘密、侵犯著作权、侵犯人身权等，请点击“版权申诉”（推荐），也可以打举报电话：400-050-0827(电话支持时间：9:00-18:30)。
查看更多
液相色谱-串联质谱法检测水果中甲维盐-食品安全质量检测学报
5 8 Vol. 5 No. 8
2014 8 Journal of Food Safety and Quality Aug. , 2014
-
*
刘丽丽, 刘 谦 , 周 杨, 白文静, 白 帆
(, 071051)
摘 要: 目的 -,
方法 , C18 , 结果 1~20
μg/L , 0.99, μg/kg 3 ,
73.9%~84.2%, 3.86%~7.53%, 0.05 μg/kg结论 ,
关键词: -; ;
Determination of emamectin in fruits by performance liquid
chromatography-tandem mass spectrometry
*
LIU Li-Li, LIU Qian , ZHOU Yang, BAI Wen-Jing, BAI Fan
(Baoding Entry-Exit Inspection and Quarantine Bureau, Baoding 071001, China)
ABSTRACT: Objective A method for the determination of emamectin in fruits by performance liquid
chromatography-tandem mass spectrometry was developed, and the sample pretreatment such as extraction,
cleanup and mobile phase were optimized. Methods The samples were extracted by acetonitrile, cleaned up
by C 18 solid phase extraction column, and determined by performance liquid chromatography-tandem mass
spectrometry. Results The linear ranges were 120 μg/L and the correlation coefficients were all above 0.99.
The recoveries of emamectin in fruits at the spiked levels of 0.1, 0.2, and 1.0 μg/kg were 73.9%84.2%. The
relative standard deviations were 3.86%7.53%. Conclusion The method can meet the requirements for the
determination of emamectin in fruits.
KEY WORDS: performance liquid chromatography-tandem mass spectrometry; emamectin; fruits
[2]
1
文档评论（0）