基于NMR技术的啤酒白酒成分分析与分类判别-电子与通信工程专业论文.docxVIP

2．4本章小结 2．4本章小结 30 第三章白酒中的微量成分分析与模型判别 ．35 3．1引言 35 3．2实验材料与方法 36 3．2．1实验样品收集与制备 ．36 3．2．2核磁共振实验条件及方法 ．36 3．2．3谱图预处理及数据建模 ．37 3．3结果与讨论 37 3．3．1白酒1H NMR实验方法优化 37 3．3．2白酒的1H NMR谱轮廓分析 38 3．3．3白酒的1H NMR谱的PCA分析 ．．40 3．3．4白酒微量成分的单变量分析 ．40 3．3．5 Fisher分类判别 ．．44 3．4本章小结 46 第四章总结与展望 51 4．1本文总结 5l 4．2展望 ．52 攻读硕士期间发表的论文 ．．55 致谢 57 万方数据 CONTE_NTSAbstract CONTE_NTS Abstract in Chinese I Abstract in EngHsh III Chapter 1 Introduction ··1 1．1 Briefintroduction ofNuclear Magnetic Resonance 1 1．2 Applications ofNMR combined with pattern recognition on food science··1 1．2。1 Data preprocessing of 1H-NMR spectrum 2 1．2．2 Pattern recognition techniques 3 1．2．3 Applications ofNMR on food science 4 1．3 Present situation and development in fiquor audy ·6 1．4 Study significance and primary contents ofthis thesis ·6 1．4．1 Significance ofthis study ··7 1．4．2 Primary contents and structure ofthis thesis ．．8 Chapter 2 Compositional quantitation and brand identification of beer via NMR approach ·1 5 2．1 Introduction ．．1 5 2．2 Materials and mahods 1 5 2．2．1 Sample collection and preparation ． 15 2．2．2 1H NMR experiment ．1 6 2．2．3 Spectrum pretreatment and data modeling 1 6 2．2．4 Quantitative analysis ofbeer composition ·17 2．2．5 Fisher discriminant model ．．1 8 2．3 Re弧lts蛆d discussion ．20 2．3．1 Analysis of 1H NMR spectrum ofbeer 20 2．3．2 PCA of 1H NMR spectrum ofbeer 22 2．3．3 Univaritate analysis ofbeer compositions ．23 2．3．4 Quantitative analysis ofbeer compositions ··25 万方数据 万方数据 万方数据 2．3．5 2．3．5 Results ofFisher discriminant ．28 2．4 Summary ．30 Chapter 3 Identification of trace composition in white spirits via NMR combined with multivariate statistical analysis． ． ． ． ．35 3．1 Introduction 一35 ：；．2 Materials and methods 36 3．2．1 Sample collection and preparation ．36 3．2．2 1H NMR experiment ．36 3．2．3 Spectrum pretreatment and data modeling 37 3．3 Results and discussion ．37 3．3．1 Optimization oflH NMR experiment ．．37 3．3．2 1H NMR