溶胶-凝胶法制备Al2O3ZrO2涂层及对γ-TiAl.PDFVIP

39 2 Vol.39, No.2 2010 2 RARE METAL MATERIALS AND ENGINEERING February 2010 -Al O /ZrO γ-TiAl 2 3 2 ( 110142) (Al(OC H ) ) (ZrOCl ·8H O) - γ-TiAl 3 7 3 2 2 Al O /ZrO 1000 2 3 2 Al O /ZrO 2 3 2 -Al O /ZrO γ-TiAl 2 3 2 TG174.44 A 1002-185X(2010)02-0367-05 TiAl (at%)12 mm×10 mm×1.5 mm 1 mm # Al2O3 1000 TiO α-Al O 2 2 3 20 g ( (C H O) Al) 98% 3 7 3 270 mL 80 1 hHNO3 MoNb W pH 3 90 5 h Ti-Al [1-3] [20] Al O 5% 2 3 Ti 20 g (ZrOCl ·8H O 2 2 [4-8] [9] 99%) 41 mL 41 mL [10][10-13] NH4OH pH 3~4 30 [14]Ti-Al 5 h 7.6% - ZrO2 10 cm/min 20 min75 [15,16]A