对动态光散射颗粒测量技术中几个问题的讨论.pdfVIP

上 海 理 工 大 学 学 报 第24 卷 第4 期 J. University of Shanghai for Science and Technology Vol.24 No.4 2002 文章编号: 1007-6735(2002)04-0313-06 对动态光散射颗粒测量技术中几个问题的讨论 郑 刚, 申 晋, 孙国强, 庄松林 (上海理工大学 光学与电子信息工程学院, 上海 200093) 摘要:在分析国内外动态光散射颗粒测量技术研究动态的基础上, 对在动态光散射颗粒测量 技术中应用的新理论和新方法, 通过增加自相关函数的拟合参数来克服热晕效应的影响, 用 单束光互相关方法提高信号的时间分辨率及测量浓悬浮颗粒时的改进装置等几个问题进行了 讨论. 关键词:颗粒测量; 动态光散射; 光子相关光谱 中图分类号: TH 74; TN 247 文献标识码:A New advance in study of particle sizing with dynamic light scattering ZHENG Gang, SHEN Jin, SUN Guo-qiang, ZHUANG Song-lin (College of Optics and Electronics Engineering, University of Shanghai for Science and Technology, Shanghai 200093, China) Abstract :Dynamic light scattering (DLS) as an important technique has been intensively researched and applied widely for more than three decades. Specially, in recent years, much significant progress has been made, such as miniature laser light scattering instrumentation for particle size analysis, modification for the thermal blooming effect to yield the correct particle size, statistical processing of photons(SPP), one-beam or two-beam cross correlation technique and use of higher order photon correlation spectroscopy to recover asymmetric spectral lineshape. Key words :particle sizing ; dynamic light scattering; photon correlation spectroscopy 动态光散射(dynamic light scattering, 简称 响测量的因素多, 所以在一些分布复杂的颗粒系 [2 , 3] DLS) 技术是进行纳米及亚微米颗粒粒径测量的 中, 很难给出令人满意的测量结果 . 国外对该