离子色谱法测定食盐中的硫酸根-食品安全质量检测学报.PDF

6 2 Vol. 6 No. 2 2015 2 Journal of Food Safety and Quality Feb. , 2015 何 攀 1,2 * ，邓洁红2 (1. 41007 2. 410128) 摘 要: 目的 方法 , , , 。结果 , 1~100 mg/L , 97.89~100.50%, 0.57%结论 , ICS3000 , , 关键词: ; ; Determination of sulfate in salt by ion chromatography HE Pan1,2*, DENG Jie-Hong2 (1.Hunan Province Product Quality Supervision and Inspection Institute, Changsha 41007, China;2.College of food science and technology,Hunan Agricultural University , Changsha 41028, China ) ABSTRACT: Objective To establish a determination methods of sulfate in salt by ion chromatography. Methods The modified gradient procedure was used to separate the sulfate standard on an anion exchange column by using silver column and nano-column as solid phase extraction column, and automatic analysis method of sulfate in salt was established. Results Under optimal experimental condition, the linear range of the sulfate was 0~100 mg/L. Standard addition recovery was 97.89~100.50%, the sulfate of salt RSD value was 0.57%. Conclusion The method base on ICS3000 ion chromatography could exclude chloride ion interference, shorten the processing time of sample, and improve the selectivity of sulfate. This method has many advantages such as simple operation, quick response, low interference, and high accuracy and sensitivity. KEY WORDS: ion chromatography; salt; sulfate