规则结构多孔炭的模板法制备与性能研究-化学工艺专业论文.docxVIP

规则结构多孔炭的模板法制备与性能研究Synthesis 规则结构多孔炭的模板法制备与性能研究 Synthesis and characterization of ordered porous carbon via a template method Abstract In this paper，we mainly focused On the preparation of ordered porous carbon materials Via a template method with commercial Y zealite as the template and furfuryI a]cohol＆propylene as carbon resources．The template method involves impregnation of carbon resource，carbonization of composite in the nano channels of the Y zeol ite and removal of framework．Effects of the synthesis parameters on the form，structure and character of the product were studi ed．X-ray diffraction(XRD)，scanning electron microscopy(SEM)，transmission electron microscopy(TEM)，Raman spectroscopy and EDX were used to study the morpho]ogies and structures of the product．Thermal stability，resistance oxidation，electric character and BET surface 8／-ea were analysed．Based on the data obtained in these investigations，mechanismS of forming porous carbon are proposed and discussed to elucidate the formation process according to preparing condi tions． It is found that，with a template method，ordered porous carbon with high surface areas can be produced with Y zeol ite and furfuryl alcohol＆propylene are separately used as template and carbon resources．Compared with those obtained product by routine chemical activated method，porous carbon obtained in our experiments have special structure and performance．The obtained porous carbons exhibi t ordered structure，high surface areas，large pore volumes and monomodal pore size distribution． SynthesiS of ordered porous carbon in this paper involves impregnation of organic carbon resources into the hole of Y ze01ite，then carbonization of composite at appropriate temperatures and final removal of framework．It is found that impregnation of organic carbon resource，best polymerization temperature and the method of dissolving the template can influence the structure and the vj eld of product． ．II． 大连理工大学硕士学位论文And 大连理工大学硕士学位论文 And alSO we founded