气相色谱-质谱联用法分析罗布麻蜂蜜中脂肪酸-食品安全质量检测学报.PDF

7 2 Vol. 7 No. 2 2016 2 Journal of Food Safety and Quality Feb. , 2016 王建梅, 刘河疆, 马玉娥, 安 冉, 孙 婷, 杨 莲* (, (), , 830091) 摘 要: 目的 -, 方法 , -, 结果 28 , (26.57%)(17.6%)(7.34%)38.83%, 61.17%结论 , , , 关键词: ; ; ; - Determination of fatty acids in Apocynum honey by gas chromatography-mass spectrometry * WANG Jiang-Mei, LIU He-Jiang, MA Yu-E, AN Ran, SUN Ting, YANG Lian (Institute of Quality Standards Testing Technology for Agro-Products, Xinjiang Academy of Agricultural Science, Laboratory of Quality and Safety Risk Assessment for Agro-Products ( Urumqi), Ministry of Agriculture , Key Laboratory of Agroproducts Quality and Safety of Xinjiang, Urmqi 830091, China) ABSTRACT: Objective To establish a method for determination of fatty acids in Apocynum honey by gas chromatography-mass spectrometry (GC-MS). Methods Fatty acids extracted by the mixture of hexane and aether were converted to methyl esters with KOH-CH OH. Then the methyl esters were determined by the area 3 normalizing method. Result There were 28 kinds of fatty acids in Apocynum honey, with the main components of linoleic acid (26.57%), pa