拉伸载荷下热障涂层体系失效分析及测试表征-材料科学与工程专业论文.docxVIP

PAGE PAGE VI 和扫描电镜(SEM)微观形貌图，探讨了常温拉伸载荷下热障涂层失效机理。 第四，组装调试万能试验机、三维变形光学无损测试系统、声发射和加热系 统，在变温环境和拉伸载荷作用下研究了 TBCs 试样界面失效过程，成功地对其 表面应变场和裂纹萌生所致的声发射信号进行实时监测。提取基底的应变数据并 代入理论解析表达式，得到了陶瓷层和粘结层的临界断裂强度分别为 64.5±6.9 MPa 和 540.5±15.2 MPa；陶瓷层/粘结层界面剪切强度和粘结层/基底界面剪切强 度分别为 26.7±2.3 MPa 和 125.6±12.5 MPa。分析断裂点的三维应变数据，获得 了陶瓷层的临界断裂强度为 61.2±3.9 MPa。对实验过程中声发射信号进行快速 傅里叶变换，得到陶瓷层表面垂直裂纹、陶瓷层/粘结层界面裂纹及粘结层垂直 裂纹的特征频谱分别为 0.28-0.30 MHz、0.07-0.09 MHz 和 0.22-0.24 MHz；借助 于扫描电镜微观形貌观察，探讨了变温拉伸载荷下热障涂层的失效模式。 关键词：热障涂层；数字图像相关法；剪滞模型；残余应力；声发射 Abstract Thermal barrier coatings (TBCs) systems have attracted an increasing attention in aircrafts and gas-turbines owing to their excellent wear resistance, corrosion resistance and thermal insulation. However, it is very difficult to validly appraise the delamination and sapllation of the top coating due to the complicated structures and service environments of TBCs, which strongly affects their life and reliabilities. In this work, the evolution of many important properties of TBCs were monitored and obtained by the aid of digital image correlation technique, acoustic emission technique and tensions. The developed measurement methods and results would be useful to predict the operation life and durability of TBCs system. On the basis of the conventional shear lag models, we have deduced a new shear lag model to analyze the interface failure of air plasma sprayed TBCs system under tensile loads at room and high temperature conditions. The main conclusions are summarized as follows, Firstly, a three-layer shear lag model has been established under considering the effect of residual stresses. An analytic solution of stress variation in the coating system was obtained based on the interface stress transferring form under external tensile loads, which was applied to predict the stress evolution of TBCs system during the fracture process. When normal strain in the substrate increase up to 0.08% and 0.11%, shear stress along the substrate/bond coat, bond coat/top coating interfa