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2 ( ) No. 2
2019 3 Journal of East China Normal University (Natural Science) Mar. 2019
: 1000-5641(2019)02-0156-08
, , , ,
( , 200241)
: - (HF-LPME-UHPLC) ,
6 . , HF-LPME
: , NaOH 0.2 mol/L,
1.0 mmol/L, Na SO 375 g/L, 30 ◦C, 300 r/min,
2 4
4 h. 6 , 6 min , ,
R2 0.998 9, 188∼950 , 0.03∼0.1 ng/mL(S/N=3).
50 µg/kg 85.2%∼95.6%, 3.13%∼4.33%
(n=5). , .
: ; ;
: O657.7 : A DOI: 10.3969/j.issn.1000-5641.2019.02.017
Determination of sulfonamides by ultra-high performance
liquid chromatography with microextraction
LI Yi, ZHANG Yan, ZHANG Ya-ting, HE Pin-gang, WANG Qing-jiang
(School of Chemistry and Molecular Engineering, East China Normal
University, Shanghai 200241, China)
Abstract: In this study, the development of an analytical method for the determination
of chicken meat based on three-phase hollow fiber membrane microextraction ultra-high
performance liquid chromatography (HF-LPME-UHPLC) was explored. A three-phase
hollow fiber membrane microextraction system was developed to optimize the extraction
conditions of HF-LPME: the extractant was n-octanol, the concentration of NaOH in the
receiving phase was 200 mmol/L, the concentration of hydrochloric acid in the sample
solution was 1.0 mmol/L, the concentration of Na SO was 375 g/L, the extraction
2 4
temperature was 30◦ , the stirring rate was 300 r/min, and the extraction time was 4 hours.
Chicken meat samples were extr
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