石墨烯复合膜修饰电极的制备与其应用分析.pdfVIP

MasterThesis ofSouthu‘estUniversity 3．4Determinationofuricacid…………………………………………………………………………………35 3．5Interference study……………………………………………………………………………………………．．36 3．6Determinationofuricacidinhumanserum…………………………………………………37 blood 4．Conclusions………………………………………………………………………………………………．．38 5．References…………………………………………………………………………………………………．38 determinationandserotonin 3Simultaneous of using Chapter dopamine sulfonic carbonelectrode．．41 glassy graphene／poly(p—aminobenzeneacid)film-coated 1．Introduction………………………………………………………………………………………………．．41 2．Experimental………………………………………………………………………………………………42 2．1 and Reagentsapparatus……………………………………………………………………………………．．42 ofthemodifiedelectrode…………………………………………………………………．43 2．2Fabrication anddiscussion．…．．．．．…．．．．．．．．．．．…．．…．…．．…．．．……．……．…．．．．．．…．…．．．．．．．．…．．…．．．．44 3．Results 3．1Characterizationofthe GR·poly(p—ABSA)／GCE…………………………………………………．44 ofDAand5．HT…………………………………………………………46 3．2Electrochemicalbehaviors ofscanrateandsolution 3．3Effects pH……………………………………………………………………46 DeterminationofDAand5．HT 3．4 concentration…………………一…………………………………48 behaviorsofDAand5-HT………………………………………．5l 3．5Effectsofinterferentsonthe 3．6 Analyticalapplications………………………………………………………………………………………52 3．7Stability…………………………………………………………………………………………………………．．53 4．Conclusions………………………………………………………………………………………………．．53 5．References．．．…．……．…．．…．．．．．．．…．．．．．．．．．…．…．…．…．．．．．．……．………．．．．．．．．．．．．……．．．．．…．．．．…．53 4 of oxide andits Ni／graphenenanocomposite