镍纳米复合材料的合成与其电催化氧化有机小分子性能分析.pdfVIP

SYNTHESISNICKELNANOCOMPOSITESANDTHEIR PROPEIU、IESONELECTROCATALYTIC0ⅪDATION0F 0RGANICSMALLMOLECULES ABSTRACT Inthis microwave methodandsolvothermalhave thesis，the method，reflux synthesis been to nanostructured ofmicrowave developedsynthesize materials．Byusing method， carbonmatrix were and graphene／nickelnanoparticle synthesized．NiS composites nano-materialswere solvothermal the Ni(OH)2 compoundedthrough synthesis．Using reflow nanowiresand nanowireswere method，nickel Ni3S2 theirelectrochemicalwerestudied．Alsothereisafoundthatnickel properties ionsinduced solvothermalof octahedral．Themaincontentsareasfollows： synthesisW03·0．5H20 1．Afacile microwave-assistedmethodfor of Ni one-step depositionmonodisperse onreduced toformNi-rGO is nanospheres grapheneoxide(rGO)sheetsnanoh)rbrids discussed．Inthe of are ontorGO presencehydrazinemonohydrate，Ninanospheresgrown sheets nickel andGOas materialsin using precursor starting ethylene underalowlevelofmicrowave 20 whichGOisalso irradiation(300W)formin，during reducedtorGO．The exhibit Ni as—preparednanohybridswell—dispersed 80nnlin andeffectivereductionof oxide．The diameter)loadings graphene resulting Ni—-rGO carbon