注射成形0Cr17Mn11Mo3N无镍高氮不锈钢的烧结.docVIP

注射成形0Cr17Mn11Mo3N无镍高氮不锈钢的烧结 第3O卷 2008定 第l0期 l0月 北京科技大学 JournalofUniversityofScienceandTechnologyBeUing VoI.3ONO.10 oct.2008 注射成形0Cr17Mn11M03N无镍高氮不锈钢的烧结 崔大伟,2曲选辉郭萍2李科 1)北京科技大学材料科学与工程学院,北京1000832)潍坊学院机电工程系,潍坊261061 摘要采用粉末注射成形技术制备了0Crl7MnllMo3N无镍高氮奥氏体不锈钢,研究了各烧结工艺参数(温度,时间,气氛) 对其相对密度及氮含量的影响.结果表明:温度是最重要的烧结参数,提高温度可以显着增加烧结体的相对密度,但引起氮含 量的下降,在1300℃以上烧结,烧结体相对密度可达99%以上;烧结时间所起作用不明显,烧结2h足够使粉末致密化过程完 成;气氛对OCrl7Mnl1MoaN不锈钢的烧结影响显着,在N2+H2混合气中烧结比在纯N2气中获得更高的相对密度及更低的 氮含量.OCrl7Mnl1Mo3N不锈钢的最佳烧结条件为:温度1300℃,时间2h,气氛采用流动的高纯氮气,此时烧结体相对密度 达到99.1%,氮质量分数为0.78%. 关键词无镍高氮不锈钢;粉末注射成形;烧结;相对密度;氮含量 分类号TF124.39:TG142.71 Sinteringofnickel-freehighnitrogen0Crl7Mnl1Mo3Nstainlesssteelpreparedby powderinjectionmolding CUIDⅡ砌ei, QuXuanhui,GUOPing.LIKe) 1)SchoolofMaterialsScienceandEngineering,UniversityofScienceandTechnologyBeijing,Beijing100083,China 2)DepartmentofMechanicalandElectronicEngineering,WeifangUniversity,Weifang261061,China ABSTRACTAkindofnickel—freehighnitrogenausteniticstainlesssteel(0Crl7MnllMo3N)waspreparedbvpowderinjection molding.Theeffectsofsinteringparameterssuchastemperature,timeandatmosphereontherelativedensityandnitrogencontent wereinvestigated.Theresultsshowthatsinteringtemperatureisthemostimportantsinteringparameter,withtheincreaseofwhich therelativedensityofsinteredspecimensincreasesremarkably,whereasthenitrogencontentdecreases ,andabove1300℃there1a— tivedensityofsinteredspecimensisover99%.Sinteringtimehasnoobviouseffectontherelativedensityandnitrogencontent. and whenthesinteringtemperatureishighenough,theexcellentdensificationofthepowdercanbeachievedwithin2h.Forthesintering of0Crl7MnllMo3Nstainlesssteel,sinteringatmospherehasalsoasignificantinfluence,andthehigherrelativedensityandlowerni— trogencontentCaDbeobtainedinN2+H2atmospherethaninhighpurityN2atmosphere.Theoptimalsinteringconditionsof 0Crl7Mnl1Mo3Nausteniticstainlesssteelareasfollows:1300℃,2h,andflowinghighpurenitrogen.Undertheoptimalcondi— tions,therelativedensityofsinteredspecimenscanreach99.1%andthemassfractionofnitrogenisash