两段式脱臭塔特性及油脂脱臭工艺条件优化.docxVIP

两段式脱臭塔特性及油脂脱臭工艺条件优化李振岚 1 ，陈晓慧 1 ，江 维 2 ，张立国 2 两段式脱臭塔特性及油脂脱臭工艺条件优化 李振岚 1 ，陈晓慧 1 ，江 维 2 ，张立国 2 ，于殿宇 1 , * (1.东北农业大学食品学院，黑龙江 哈尔滨 150030； 2.哈尔滨工大高新技术产业开发股份有限公司中大植物蛋白分公司，黑龙江 哈尔滨 150038) 摘 要：对板式脱臭塔进行改造，采用外部加热的方式，进行两段式脱臭，将脱色油通过双螺旋加热器加热到 1 70 ℃，使其进入上段板式塔，经初步汽提后的油引出脱臭塔，进入残压 2 T o rr 的双螺旋加热器加热到 248℃， 然后进入下段板式塔蒸馏。脱臭过程中上段脱臭塔中蒸汽用量为油质量的 1%，下段脱臭塔中蒸汽用量为油质量的 2%，脱臭时间 45min，油在脱臭塔中滞留的时间大大缩短，油脂中反式脂肪酸相对含量仅为 1.15%，是一种绿色、 节能的新型脱臭设备。 关键词：大豆油；两段式脱臭；残压；反式脂肪酸 Characteristics of Two-stage Deodorizer and Optimization of Oil Deodorization LI Zhen-lan1，CH EN Xiao -hu i1，JIA NG Wei2，ZHA NG L i-gu o2，YU Dian-y u1, * (1. School of Food Science, Northeast Agricultural University, Harbin 150030, China； 2. Harbin Gongda High-tech Enterprise Development Co. Ltd., Zhongda Plant Protein Branch, Harbin 150038, China) Abstract ：In this study, tray type deodorizer was modified by external heating strategy to achieve two-stage deodorization. In this deodorization process, decolorized soybean oil was heated by double-helix heater to the optimal temperature of 170 ℃. After the oil entered the upper section of tray type column, primary gas stripping was carried out. Then, the oil was again transferred to double-helix heater where the residual pressure was set at 2 Torr and heated to 248 ℃ before distillation in the bottom section of tray type column. Steam amount in the upper section of tray type column represented 1% of total oil weight and in the bottom section 2%, and the total deodorization time was set at 45 min. As a result, oil retention time in deodorizer was largely shortened and the trans-fatty acids content in soybean oil was only 1.15%. Therefore, two-stage deodorizer reveals pollution-free and energy-saving properties. Key w ords：soy bean o il；two-stage deodorization；residual pressu re；trans-fatty acids 中图分类号：TS224.6 文献标识码：A 文章编号：1002-6630(2011)14-0139-05 反式脂肪酸(trans fatty acids，TFA)，是所有含有 反式非共轭双键的不饱和脂肪酸的总称，包括单不饱和 反式脂肪酸和多不饱和反式脂肪酸，其空间构象呈线 性，性质接近饱和脂肪酸[ 1 - 2 ] ，通常顺式脂肪酸多为液 态，熔点较低；反式脂肪酸多为固态或半固态，熔点 较高