毕业设计（论文）-4000ta乙胺生产装置分离工段的工艺设计.doc

摘 要 乙胺包括一乙胺、二乙胺、三乙胺，目前生产乙胺的方法有很多种，其中的乙醇氨解法具有工艺先进、无副反应、产品质量高、能耗低，能同时生产一乙胺、二乙胺、三乙胺等的优点。 本次设计是对4000 t/a 乙胺生产装置分离工段的工艺设计。根据各物料挥发度的不同以及三乙胺与乙醇、水的三元共沸物在不同压力下共沸组成的不同，对乙胺粗产品进行了分离。乙胺分离系统包括6个塔，精馏后得到纯的一乙胺、二乙胺、三乙胺产品。利用模拟软件AspenPlus对乙基胺分离系统进行了设计和模拟计算，得到了各塔理论板数和回流比等设计参数。 设备选型计算中根据处理任务要求，对主要设备进行了选型。列出了设备一览表。最后用CAD绘制了物料流程图、带控制点的工艺流程图和绘制厂区平面布置图。 关键词：乙胺；工艺设计；Aspen Plus模拟流程 全套图纸加扣?3012250582  Abstract Ethylamine, including ethylamine, diethylamine, triethylamine, the current production of ethylamine are many ways, one of the ethanol ammonia solution with advanced technology, no side effects, high product quality, low energy consumption, can produce a Ethylamine, diethylamine, triethylamine and the like. Process design of separation section of 4000t/a ethylamine production plant. Triethylamine, ethanol and water form a triple azeotropic system whose composition changes according to the pressure because the volatility of each component in the system is not the same.Because of this, amixture of ethylamines can be separated by distillation.Pure ethylamine, diethylamine and triethylamine were separated using six distillation towers. We designed and simulated the ethylamine separation system using AspenPlus.The optimal parameters such as theoretical plate number and reflux ratio were obtained. Equipment selection calculation according to the processing requirements, the main equipment was selected The Lists the equipment list. Finally, drawing the material flow chart,the control point of the process flow chart and the factory layout plan with CAD. Key words: ethylamine; process design; Aspen Plus simulation process 目 录 TOC \o "1-3" \f \h \z 第1章 乙胺生产方案的论证 1 6972 1.1 乙胺的性质 1 8339 1.2 乙胺的用途 1 5574 1.3 乙胺的市场需求预测 2 4986 1.3.1国外乙胺产能及需求预测 2 31657 1.3.2国内乙胺产能及需求预测 2 29612 1.4 乙胺生产中节能方案的探讨 4 15519 第2章 乙胺生产方案的论证 5 18110 2.1生产方案的介绍 5 20906 2.2 工艺方案的确定 6 27774 第3章 工艺流程说明 7 739 3.1 工艺流程概述 7 32262 3.2