pH计安装调试与维护.pptVIP

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* * KEY SLIDE Message: the customer’s needs grow and only a good sensor is not enough anymore Examples see green frames How to win? – read arrow: we have to understand and adapt – therefore ISM * * * The fundamentals of our ISM technology that you know already are always the same We want to simplify all the operations around the measurement loop like installation, * The fundamentals of our ISM technology that you know already are always the same We want to simplify all the operations around the measurement loop like installation, * * * * * * * * Need 6 things to calibrate an electrode 1) the electrode 2) + 3) two buffers 4) wash bottle/bucket of water 5) tissues 6) thermometer Explain why 6) is important - buffer tables Tissues help get water out of housing Do not rub, creates static electricity. Talk about buffers and need to use CO2-free water if making buffers from concentrate or dry chemicals. Do not buy buffers in too large volumes - false economy, 慻o off?once opened. * * * Remember from Nernst equation that temperature is involved. Will look at under these headings 1) effect of temperature on the solution itself 2) the Nernstian effect 3) ................... 4)..................... * The MOST IMPORTANT thing you can do to ensure reliable pH measurement * Dry - causes pH glass to dry and become non-functional Sore in electrolyte NOT distilled water - why? Draw schematic of diaphragm and effect of osmolarity difference on diaphragm. - increased impedance - unstable diaphragm potential - for electrodes with AgCl saturated electrolyte dilution of electrolyte causes dissociation of argentohalide complexes and precipitation of AgCl in the diaphragm resulting in blockage. * * * 传感器耗损度: 如何实现 传感器所经历的条件如SIP、CIP、高温、极端的pH值都记录在芯片中,通过这个模型算出传感器的耗损度。 有效的老化时间 有效的 SIP/CIP 老化模型 温度如何影响pH测量? 电极斜率 电极使用寿命 电极响应时间 太热了! 请注意 保持隔膜清洁! 电极的清洗 一般污染:使用水、 0.1MNaOH或0.1MHCl清洗电极数分钟; 油脂或有机物的污染:用丙酮或乙醇清洗电极数秒钟 蛋白质污染(隔膜变黄):将电极用9891清洗液处理 (订货号250ml); 硫化物污染(隔膜变黑

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