乙酸乙酯的反应器设计作业流程.doc

摘 要 乙酸乙酯是一类关键有机溶剂和有机化工基础原料，其用途很广泛，现在中国采取传统方法制备即乙酸和乙醇为原料，浓硫酸为催化剂直接催化合成乙酸乙酯。所以经过对乙酸乙酯理化性质，社会用途和需求和中国外发展现实状况进行研究调查和乙酸乙酯在试验室制法和工业生产各方面对比以后，为此对乙醇和乙酸缩合进行了乙酸乙酯合成工艺课程设计。本选题为年产量为年产5017吨乙酸乙酯反应器设计 。对工业生产中物料衡算，热量衡算和合成工艺设备等方面为间歇釜式反应器工业设计提供较为详尽数据和图纸。本选题为年产量为年产5017吨乙酸乙酯反应器设计 。 关键字：乙酸；乙醇；乙酸乙酯；合成工艺；间歇式反应器 Abstract Ethyl acetate is a kind of important organic solvents and basic organic chemical raw materials, its application is very broad, our country prepared using traditional methods that acetic acid and ethanol as raw material, concentrated sulfuric acid catalyzed direct synthesis of ethyl acetate. So through the social use of physical and chemical properties of ethyl status quo needs, and conduct research and development at home and abroad as well as various aspects of ethyl acetate after comparing laboratory and industrial production system of law, for the condensation of ethanol and acetic acid were synthesis of ethyl curriculum design. The topic for the annual production of 5,017 tons annual output of ethyl reactor design. In industrial production of material balance, heat balance and synthesis process equipment to provide more detailed data and drawings for the batch tank reactor industrial design. The topic for the annual production of 5,017 tons annual output of ethyl reactor design. Key words:?Acetic acid; Ethanol; Ethyl acetate; Synthesis process; Batch reactor 目 录 TOC \o "1-3" \h \z \u 摘 要 Ⅰ Abstract Ⅱ 第一章 前 言 8 1.1 乙酸乙酯概述 8 1.1.1 乙酸乙酯介绍 8 1.1.2 乙酸乙酯用途 8 1.1 乙酸乙酯产能和市场需求 9 1.2.1 世界乙酸乙酯产能和消费情况 9 1.2.2 中国乙酸乙酯产能和消费情况 9 第二章 工艺步骤比较 12 2.1 本课题设计内容和要求 12 2.1.1 设计要求 12 2.1.2 具体设计内容 12 2.2 设计方案确实定 12 2.2.1反应原理 12 第三章 工艺设计方案 14 3.1原料路线确定标准和依据 14 3.1.1乙醇乙酸酯化法 14 3.1.2乙醛缩正当 14 3.1.3乙烯加成法 15 3.1.4乙醇脱氢法 15 第四章 工艺设计计算 17 4.1 设计依据 17 4.2设计方案 17 4.3设计条件 17 4.4反应条件 17 4.5工艺计算及方案选择 17 4.5.1反应器操作有间歇操作和连续操作 17 4.5.2间歇反应釜进料 18 4.5.3 流量计算 18 4.5.4 反应体积及反应时间计算 19 4.6连续性反应釜进料计算 20