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chemical analysis method Classical methods : (also known as wet chemistry methods) Use separations such as precipitation, extraction, and distillation and qualitative analysis by color, odor, or melting point. Quantitative analysis is achieved by measurement of weight or volume. Analytical methods : Classical and Instrumental Instrumental methods: Use an apparatus to measure physical quantities of the analyte such as light absorption, fluorescence, or conductivity. The separation of materials is accomplished using chromatography or electrophoresis methods. Although modern analytical chemistry is dominated by sophisticated instrumentation, the roots of analytical chemistry and some of the principles used in modern instruments are from traditional techniques many of which are still used today. These techniques also tend to form the backbone of most undergraduate analytical chemistry educational labs. Classification Gravimetric analysis Involves determining the amount of material present by weighing the sample before and/or after some transformation. Application:moisture、ash、fat、DF (dietary fiber)、pectin Volumetric analysis Titration involves the addition of a reactant to a solution being analyzed until some equivalence point is reached. Different titrations may use different types of indicators to reach some equivalence point. Application: acid base titration Total acid , protein, benzoic acid oxidation-reduction titration reducing sugar Titration mode Direct titration Back titration Replacement titration Indirect titration MOISTURE DETERMINATION Teaching Aims The significance of determination of moisture The principle and the methods of moisture determination How to improve the accuracy and precision in moisture determination What’s the significance of moisture determination? * Moisture Determination Moisture or water is by far the most common component in foods ranging in content from 60 ~ 95%. The two most common moisture
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