年产1000吨氨基乙酸生产工艺设计.docx

学士学位论文（设计） 题目： 年产1000吨氨基乙酸生产工艺设计 姓 名 学 号 院 系 专 业 指导教师 年 月 日 PAGE PAGE II 摘 要 氨基乙酸别名甘氨酸，它是α-氨基酸中结构最简单的，它有十分广泛的应用，包括用于灭草剂、医疗药品、食品、饲料和用于生产其它氨基酸，合成表面活性剂等。氨基乙酸的生产方式有很多种，最主要的有氯乙酸氨解法和施特雷克法。在我国，基于工艺、主要原材料等原因，多数选用氯乙酸氨解法。本设计的主要目的是为了对模拟年产1000吨氨基乙酸的厂房工艺采取设计和进一步优化，本设计简单介绍了氨基乙酸的主要用途，国内外的生产情况，研究进展和未来的发展趋势。根据我国的自身情况，本设计选取了氯乙酸氨解法，选取间歇式的生产方式，初步设计要求年产值量1000吨，参考了许多文献及相关数据，对整体的生产过程做了物料衡算，主要设备完成了热量衡算，并对核心设备氨化合成釜进行了设计，对生产技术流程完成了改进，对车间进行了布设和优化。 关键词：氨基乙酸；生产工艺；收率；氯乙酸氨解 ABSTEACT Glycine is the most simple structure of the α-amino acids,its use is very extensive,mainly for agricultural chemicals,pharmaceuticals,food,feed and other production of amino acids,synthetic surface-active agent.There are many methods of producing lycine.The main solutions are ammonia and Chloroacetate Streck law. At home, because of technology, raw materials and other reasons,most plants use chloroacetic acid ammonolysis process . The purpose of the design is to optimize the workshop process of an annual output of 1,0000 tons of Glycine .The design gives a briefing on the process of the main purposes of glycine, the situation of the production at home and abroad,the research progress and future development trends. With the actual situation development in China, the design chose the chloroacetic acid ammonolysis process and use the intermittent mode of production.The preliminary design requirements of annual 10,000 tons, Searched a number of documents and data，did the material balance of the entire production process the heat balance of the major equipment,designed the main equipment amination of reactor , optimized the production process. After we repeated modifications and adjustments,we got many data and be able to get control of the process parameters, which are theoretically in line with the product of the design requirements. Key Words：glycine; production process; yield; chloroacetic acid a