关机注意事项.pdfVIP

Shutting down the system Buffers left in the system can precipitate and damage instrument components. Buffers dissolved in water may precipitate You may want to shut down the system between analyses, overnight or for a weekend, or for 72 hours or more. Tip: If you are using Empower software to control the system, set system shutdown parameters in the Instrument Method Editor. Consult the Empower Help for more information. If you are using MassLynx software to control your system, set system shutdown parameters in the Shutdown Editor. Consult the MassLynx Help for more information. Between analyses To shut down the system between analyses: 1. Between analyses, continue to pump the initial mobile phase mixture through the column. This maintains the column equilibrium necessary for good retention time reproducibility. 2. If a few hours will pass before the next injection, slow the flow rate in the interim to a few tenths of a mL/min to conserve solvent. Tip: Ensure that Auto-Shutdown for your shutdown method is deactivated. 3. Keep the detector operating, and the column manager at operating temperature, during this period. Overnight or weekends To shut down the system overnight or over a weekend: 1. Flush the column with 1:1 mixture of methanol/acetonitrile. This maintains the column bed in an active, wetted state. Requirement: If you are using buffers, you must first flush the column with a high water content mobile phase (90% H2O). Then stop the pump flow. 2. If possible, extinguish the detector lamp to lengthen lamp life. 3. The column manager can operate overnight but should be shut down over the weekend. Caution: The power switch on each system instrument controls the basic operational state of that instrument. A portion of the instrument remains powered- on after the instrument is switched off. To completely interrupt power to a system instrument, set the power swit