DB43_T 2192-2021 水环境中人口标记物可替宁含量的测定 液相色谱-串联质谱法.docxVIP

ICS?19.020 CCS?N?50  43 湖 南 省 地 方 标 准 DB43/T?2192—2021 水环境中人口标记物可替宁含量的测定 液相色谱-串联质谱法 Determination?of?population?marker?cotinine?in?water?environment with?liquid?chromatography-tandem?mass?spectrometry 2021?-?11?-?09?发布 2022?-?01?-?09?实施 湖南省市场监督管理局 发?布 DB43/T?2192—2021 目 次 前言························································································································?Ⅲ 1 范围?·····················································································································?1 2 规范性引用文件?······································································································1 3 定义?·····················································································································?1 4 方法原理?···············································································································1 5 试剂和材料?············································································································1 6 仪器和设备?············································································································2 7 样品制备和保存?······································································································3 8 分析步骤?···············································································································3 9 结果计算与表示?······································································································6 10 方法检出限和定量限?······························································································?6 附录?A（资料性）?可替宁(Cotinine）及其氘代内标的?MRM?色谱图············································7 I DB43/T?2192—2021 前 言 本文件按照?GB/T?1.1—2020《标准化工作导则 第?1?部分：标准化文件的结构和起草规则》的规 定起草。 请注意本文件的某些内容可能涉及专利。本文件的发布机构不承担识别专利的责任。 本文件由湖南省市场监督管理局提出并归口。 本文件起草单位：湖南省产商品质量检验研究院和湖南省毒品检验分析室（长沙市公安局毒品检验 鉴定中心）。 本文件主要起草人：刘红梅、肖蓉、李欣、张旭东、陆世雄、钱荣敬、张蕾、唐超群、陈实、叶小 兰、李志丰。 III DB43/T?2192—2021 水环境中人口标记物可替宁含量的测定 液相色谱-串联质谱法 1??范围 本文件规定了水环境样品中可替宁的测定方法。 本文件适用于水环境样品中可替宁含量的