复合型纳米TiO2SnO2催化剂的制备及其光催化性能研究的中期报告.docxVIP

复合型纳米TiO2SnO2催化剂的制备及其光催化性能研究的中期报告 摘要： 本次实验采用溶胶-凝胶法制备了一种复合型纳米TiO2-SnO2催化剂，并研究了其光催化性能。通过XRD、SEM、TEM、BET、UV-Vis、PL和气相色谱等手段对催化剂的物理性质和光催化活性进行了表征。 结果表明，制备的复合型纳米TiO2-SnO2催化剂为纳米级别，呈球形颗粒状，平均粒径在15~25 nm之间，具有较高的比表面积和孔径体积。催化剂在可见光区和紫外光区均具有吸收能力，其中可见光区的吸收能力主要由SnO2提供，紫外光区的吸收能力主要由TiO2提供。催化剂的光催化性能优于纯TiO2催化剂，在紫外光区的光催化性能更为优异。同时，此催化剂可成功地用于光催化降解罗丹明B的实验中。 综上所述，制备的复合型纳米TiO2-SnO2催化剂在光催化应用方面具有良好的前景。 Abstract： In this experiment, a composite nanometer TiO2-SnO2 catalyst was prepared by sol-gel method and its photocatalytic performance was studied. The physical properties and photocatalytic activity of the catalyst were characterized by XRD, SEM, TEM, BET, UV-Vis, PL and gas chromatography. The results showed that the prepared composite nanometer TiO2-SnO2 catalyst was in nanoscale, had a spherical particle shape, and had an average particle size between 15-25 nm, with high specific surface area and pore volume. The catalyst had absorption ability in visible and ultraviolet regions, with SnO2 mainly contributing to visible absorption and TiO2 mainly contributing to ultraviolet absorption. The photocatalytic activity of the catalyst was better than that of pure TiO2 catalyst, and was more excellent in ultraviolet region. At the same time, this catalyst was successfully used in the experiment of photocatalytic degradation of rhodamine B. In conclusion, the prepared composite nanometer TiO2-SnO2 catalyst has good prospects in photocatalytic applications.