《工业分析 Industrial Analysis》课件——葡萄糖旋光度的测定（双语）.pptxVIP

项目八：常规物理常数与性能分析任务六：旋光度的测定葡萄糖旋光度的测定课程：工业分析中文

Scenario8:PhysicalconstantsandperformancetestingTask6:DeterminationofopticalrotationDeterminationofglucoserotationCourse:IndustrialAnalysisEglish

1、常用的旋光仪一、测定仪器圆盘旋光仪WZZ-1型旋光仪WZZ-2型旋光仪本次实验用中文

1、Commonlyusedpolarimeters一、measuringinstrumentDiskpolarimeterWZZ-1polarimeterWZZ-2polarimeterusedinthisexperimentEglish

2、圆盘旋光仪的构造原理光源起偏镜偏振光盛液管旋转后的检偏镜通过检偏镜偏振光的偏振光中文

2、TheconstructionprincipleofadiscpolarimeterLightsourcepolarizingmirrorpolarizinglightliquidtubePolarizedlightafterrotationAnalyzerPolarizedlightthroughaanalyzercrystalaxiscrystalaxiseyepieceEglish

3、测定时的现象三分视场变化示意图中文

3、PhenomenaduringmeasurementSchematicdiagramofchangesinthethree-wayfieldofviewBeforeputtingintherotatorymaterial,adjustthescalehandwheeltomaketheilluminanceofthethreeviewingfieldsconsistent,andreadthecursorreadingThechangesinthethree-wayfieldofviewafterinsertingopticalmatterRotatethepolarizingmirrortorediscovertheconsistentilluminanceofthethreepartsfieldofview,andreadthevernierreadingEglish

4、测定注意事项测定前以溶剂作空白校正，测定后，再校正一次，以确定测定时零点有无变动；如第二次校正时发现零点有变动，应重新测定旋光度。配制溶液及测定时，应调节温度为20±0.5℃（或各药品项下规定的温度）供试的液体或固体药物的溶液应不显浑浊或含有混悬的小颗粒，如有上述现象，应预先过滤，并弃去初滤液。中文

4、NoteBeforemeasurement,useasolventforblankcalibration.Aftermeasurement,calibrateagaintodetermineifthereisanychangeinthezeropointduringmeasurement;Ifthereisachangeinthezeropointduringthesecondcalibration,therotationshouldberemeasured.Whenpreparingsolutionsandconductingmeasurements,thetemperaturesho