草莓中多种农药残留检测能力验证结果与分析.pdfVIP

分析检测

草莓中多种农药残留检测能力验证结果与分析

112*3

莫秋岸，林爱琴，唐帅，常虹

（1.海南省检验检测研究院儋州分所，海南儋州571737；2.海口市秀英区妇幼保健站，海南海口570311；3.海南省检

验检测研究院，海南海口570311）

摘要：目的：对草莓中多种农药残留检测能力验证过程及结果进行分析，为其他实验室精准测定多种

农药残留提供参考。方法：样品经QuEChERS前处理，采用气相色谱-质谱联用法和高效液相色谱法-质谱

联用法定量分析。结果：能力验证采用的方法重复性好，质控方式有效，结果稳定可靠。能力验证结果|Z|

值在0～0.6，结果令人满意。结论：农药残留检测能力验证过程中，应注重质量控制，确保获得准确的检

测结果。

关键词：农药残留；检验检测；能力验证；结果分析

ProficiencyTestingResultsandAnalysisofMultiplePesticide

ResiduesinStrawberries

112*3

MOQiuan,LINAiqin,TANGShuai,CHANGHong

(1.DanzhouBranchofHainanProvincialInspectionandTestingResearchInstitute,Danzhou571737,China;

2.HaikouXiuyingDistrictMaternalandChildHealthStation,Haikou570311,China;

3.HainanProvincialInspectionandTestingResearchInstitute,Haikou570311,China)

Abstract:Objective:Toanalyzethevalidationprocessandresultsoftheabilitytodetectmultiple

pesticideresiduesinstrawberries,andprovidereferenceforotherlaboratoriestoaccuratelydeterminemultiple

pesticideresidues.Method:ThesamplewaspretreatedwithQuEChERSandquantitativelyanalyzedusinggas

chromatography-massspectrometryandhigh-performanceliquidchromatography-massspectrometry.Result:The

methodusedforproficiencytestinghasgoodrepeatability,effectivequalitycontrolmethods,andstableandreliable

results.Theresultsoftheabilityverificationshowthatthe|Z|valuerangesfrom0to0.6,whichissatisfactory.

Conclusion:Duringtheverificationprocessofpesticideresiduedetectioncapability,qualitycontrolshouldbe

emphasizedtoensureaccuratedetectionresultsareobtained.

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