国外标准分享ASTM E967.docxVIP

Designation:E967–03

StandardTestMethodfor

TemperatureCalibrationofDifferentialScanning

1

CalorimetersandDifferentialThermalAnalyzers

Thisstandardisissuedunderthe?xeddesignationE967;thenumberimmediatelyfollowingthedesignationindicatestheyearof

originaladoptionor,inthecaseofrevision,theyearoflastrevision.Anumberinparenthesesindicatestheyearoflastreapproval.A

superscriptepsilon(e)indicatesaneditorialchangesincethelastrevisionorreapproval.

1.Scope

1.1Thistestmethoddescribesthetemperaturecalibration

ofdifferentialthermalanalyzersanddifferentialscanning

calorimetersoverthetemperaturerangefrom?40to+2500°C.

1.2Computerorelectronicbasedinstruments,techniques,

ordatamanipulationequivalenttothistestmethodmayalsobe

used.

4.SummaryofTestMethod

4.1Thistestmethodconsistsofheatingthecalibration

materialsatacontrolledrateinacontrolledatmosphere

througharegionofknownthermaltransition.Theheat?ow

intothecalibrationmaterialorthedifferenceoftemperature

betweenthecalibrationmaterialandareferencesampleanda

referencematerialismonitoredandcontinuouslyrecorded.A

transitionismarkedbytheabsorptionofenergybythe

specimenresultinginacorrespondingendothermicpeakinthe

heatingcurve.

1.3SIunitsarethestandard.

1.4ThistestmethodissimilartoISOstandard11357–1.

1.5Thisstandarddoesnotpurporttoaddressallofthe

safetyconcerns,ifany,associatedwithitsuse.Itisthe

responsibilityoftheuserofthisstandardtoestablishappro-

priatesafetyandhealthpracticesanddeterminetheapplica-

bilityofregulatorylimitationspriortouse.Speci?cprecau-

tionarystatementsaregiveninSection7.

N1—Heat?owcalibrationsaresometimesdeterminedinconjunc-

OTE

tionwithtemperaturecalibration.Somedifferentialscanningc