国外标准分享ASTM E1356.docxVIP

Designation:E1356–03

StandardTestMethodforAssignmentofthe

GlassTransitionTemperaturesbyDifferentialScanning

1

Calorimetry

Thisstandardisissuedunderthe?xeddesignationE1356;thenumberimmediatelyfollowingthedesignationindicatestheyearof

originaladoptionor,inthecaseofrevision,theyearoflastrevision.Anumberinparenthesesindicatestheyearoflastreapproval.A

superscriptepsilon(e)indicatesaneditorialchangesincethelastrevisionorreapproval.

1.Scope

ScanningCalorimetersandDifferentialThermalAnalyz-

ers2

1.1Thistestmethodcoverstheassignmentoftheglass

transitiontemperaturesofmaterialsusingdifferentialscanning

calorimetryordifferentialthermalanalysis.

1.2Thistestmethodisapplicabletoamorphousmaterialsor

topartiallycrystallinematerialscontainingamorphousregions,

thatarestableanddonotundergodecompositionorsublima-

tionintheglasstransitionregion.

1.3Thenormaloperatingtemperaturerangeisfrom?120to

500°C.Thetemperaturerangemaybeextended,depending

upontheinstrumentationused.

1.4Computerorelectronic-basedinstruments,techniques,

ordatatreatmentequivalenttothistestmethodmayalsobe

used.

E1142TerminologyRelatingtoThermophysicalProper-

ties2

2.2ISOStandard:

11357–2DifferentialScanningCalorimetry(DSC)-Part2

DeterminationofGlassTransitionTemperature3

3.Terminology

3.1De?nitions:

3.1.1Thefollowingtermsareapplicabletothistestmethod

andcanbefoundinTerminologyE473andTerminology

E1142:differentialscanningcalorimetry(DSC);differential

thermalanalysis(DTA);glasstransition;glasstransition

temperature(Tg);andspeci?cheatcapacity.

3.2De?nitionsofTermsSpeci?ctoThisStandard:

3.2.1Therearecommonlyusedtransitionpointsassociated

withtheglasstransitionregion.—(SeeFig.1.)

extrapolatedendtemperature,(Te),°C—thepointof

int