iNbTaZr形状记忆合金塑性变形微观结构的研究.doc

PAGE TiNbTaZr形状记忆合金塑性变形微观结构分析 摘 要 形状记忆合金是近几十年发展起来的一种新型功能材料，也是当代新材料研究的热点之一。本试验制备不同变形量的TiNbTaZr合金试样，通过 X射线衍射分析、透射电子显微分析、能谱仪分析、硬度测试研究TiNbTaZr合金的显微组织和相结构，分析变形量对显微组织、相结构以及织构的影响。得到如下结论。 TiNbTaZr材料具有良好的塑性，在变形量达到90%多时，仍有很好的韧性。试样的硬度随着轧制变形量的增大而提高。由X射线衍射图可知，材料在轧制变形过程中，由于不同变形量的试样峰的位置基本不变所以没有新相生成，但不同变形量的峰值强弱不同所以有织构产生。由透射电子显微分析可知，该材料室温金相为立方晶系TiNb相结构，晶胞参数为a＝3.286，随着变形量的增大晶胞参数有所减小。9同变形量织构随变形量的增加而增加，同一变形量织构主要集中于（200）晶面。 关键词：TiNbTaZr，塑性变形，显微组织，晶体结构，织构 Study of Shape Memory Alloy TiNbTaZr ABSTACT Shape memory alloy is developed in recent decades a new type of functional materials, new materials, contemporary research is one of the hotspots. xperiment with different deformation TiNbTaZr prepared alloy samples with different deformation through the hardness of analysis, differential thermal analyzer test phase transition point, X-ray diffraction, scanning electron microscopy and energy dispersive analysis and transmission electron microscope to study the TiNbTaZr alloy microstructure and phase composition of alloy element on the microstructure. TiNbTaZr material has good plasticity, the deformation of 90% for a long time, there is still a very good toughness. The hardness of the sample with the increase of rolling reduction increased. By the X-ray images that the material deformation in the rolling process, due to different deformation of the sample peak position is essentially the same, there is no new phase formed, but the peak intensity of different deformation texture produced different so there. By the transmission electron microscopy that the material gold cubic phase at room temperature NbTi martensitic structure, with cell parameters a = 3.286, as the deformation increases the unit cell parameters decreased. Different deformation of the crystal microstructure changes, with the increase of crystal deformation dislocations appear and lath martensite. As the rolling deformation texture produced by the organization known composition, different deformation texture with the increas