低品位红土镍矿制备镍精矿的试验研究.docVIP

第 44 卷第 1 期 2013 年 1 月  中南大学学报(自然科学版) Journal of Central South University (Science and Technology)  Vol.44 No.1 Jan. 2013  低品位红土镍矿制备镍精矿的试验研究 朱德庆 1 ，郑国林 1 ，潘建 1 ，李启厚 2 ，安月明 3 ，朱景和 3 ，刘志宏 2 (1. 中南大学资源加工与生物工程学院，湖南长沙，410083； 2. 中南大学冶金科学与工程学院，湖南长沙，410083； 3. 中国有色矿业集团有限公司，北京，100029) 摘要：对某低品位腐殖土型红土镍矿(镍和铁质量分数分别为 1.01%和 15.72%)进行压块—还原焙烧—磁选试 验，研究还原温度、还原时间、复合添加剂用量和预热温度对镍和铁回收效果的影响。研究结果表明：在碱度(即 CaO 与 SiO2 质量比)为 0.2、复合添加剂质量分数为 14%、预热温度为 900 、预热时间为 15 min、还原温度为 1 250 、还原时间为 35 min、煤与矿质量比为 2.7、磨矿细度小于 0.074 mm 的质量分数为(95±4)%、磁选磁场强 度为 131.34 kA/m 的条件下，获得镍和铁品位分别为 4.22%和 69.75%的镍精矿，镍和铁回收率分别为 92.22%和 85.73%；适宜的预热制度有利于团块中镍、铁的富集；复合添加剂促进了镍铁晶粒的聚集、长大，提高了镍、铁 回收效果。 关键词：腐殖土型红土镍矿；直接还原；复合添加剂；镍精矿 中图分类号：TF815；TF803.12 文献标志码：A 文章编号：1672?7207(2013)01?0001?07  Study of producing nickel concentrate from low-grade laterite ore ZHU Deqing 1 , ZHENG Guolin 1 , PAN Jian 1 , LI Qihou 2 , AN Yueming 3 , ZHU Jinghe 3 , LIU Zhihong 2 (1. School of Minerals Processing and Bioengineering, Central South University, Changsha 410083, China? 2. School of Metallurgical Science and Engineering, Central South University, Changsha 410083, China? 3. China Nonferrous Metal Mining (Group) Co. Ltd., Beijing 100029, China) Abstract: The enrichment of Ni from a low-grade saprolite laterite assaying with 1.01% Ni and 15.72% Fe was studied through briquetting—reduction—magnetic separation process and the effects of reduction temperature, reduction duration, dosage of composite additive, preheating temperature on the recovery of Ni and Fe were examined to optimize the process. The results show that nickel concentrate with 4.22% Ni and 69.75% Fe was achieved with recoveries of 92.22% and 85.73% for Ni and Fe respectively at the following conditions: basicity (mass ratio of CaO to SiO2) 0.2, dosage of composite additive 14%, preheating at 900℃ for 15 min, reduction at 1 250 ℃ for 35 min, mass ratio of coal to ore 2.7, grinding fineness of (95±4)% passing 0.074 mm and magnetic