进出口食品中高氯酸盐的测定英文意见稿.docVIP

ICS SN 中华人民共和国出入境检验检疫行业标准 XX/T XXXXX—XXXX 进出口食品中高氯酸盐的测定 液相色谱-质谱/质谱法 Determination of perchlorate in foods for import and export –LC/MS/MS Method （本稿完成日期：2012.05.20） XXXX - XX - XX发布 XXXX - XX - XX实施 中华人民共和国国家质量监督检验检疫总局发布 Foreword This standard was drafted in accordance with the GB/T 1.1-2009. It is noted that some contents in this file may involve in patent authority.Agency regarding distribution and publication of this file does not be responsible for the identification of these patents. This standard was proposed by and was under the charged of National Regulatory Commission for Certification and Accreditation. This standard was drafted by Guangdong Entry-Exit Inspection and Quarantine Bureau of the People’s Republic of China. This standard was mainly drafted by Wu yingxuan，Lin feng, Shao linzhi ,ou yang shaolun,yao yangxun and lu li. Determination of perchlorate in foods for import and export –LC/MS/MS Method Scope This standard specifies the method of determination and confirmation of perchlorate in foodstuffs by LC-MS/MS. This standard is applicable for the determination of perchlorate in water , fruit , milk , power , grain , aquatic products , animal tissue. Quoted normative documents The following normative documents contain provisions which, through reference in this text, constitute provisions of this Professional Standard. For dated references, subsequent amendments to, or revisions of, any of these publications do not apply. However, parties to agreements based in this Professional Standard are encouraged to investigate the possibility of applying the most recent editions of the normative documents indicated below. For undated references, the latest edition of the normative document referred to applies. GB/T 6682 Water for analytical laboratory use-Specification and test methods. Principle Perchlorate in the sample is extracted with 1% acetic acid in water .The acetonitril makes it less cloudy.The extraction solution is cleaned by passing