溶胶-凝胶法制备掺杂TiO2粉体及其性能的研究.docVIP

学校代码：11059 学号 Hefei University 毕业设计（论文） BACHELOR DISSERTATION 论文题目学位类别学科专业作者姓名导师姓名完成时间2014/5/23  溶胶-凝胶法制备掺杂TiO2粉体及其性能研究 摘 要 关键词 ：二氧化钛；掺杂；光催化；甲基橙溶液  Sol-gel method doped TiO2 powders and its performance study ABSTRACT In recent years, as a kind of photocatalyst TiO2 in the field of environmental governance plays a very important role, showing a great application prospect, however, TiO2 has wide band gap (3.2 eV), can only stimulate its photocatalytic activity under uv irradiation, the ultraviolet light accounts for only about 4% of the total solar radiation energy, so the sun can be the visible light cant be effectively used. Therefore, improve the utilization rate of TiO2 catalyst to visible light and improve its photocatalytic quantum efficiency has become an important task in the field. Currently, improved the method of TiO2 photocatalytic performance main have semi conductor after us, from doping, the gold is mixing complex and expensive metal deposition, etc. In this paper, using sol-gel method doped molybdenum ion of nanometer TiO2 photocatalyst, XRD, electron microscope and other instruments on the analysis of its structural morphology were characterized and the degradation of methyl orange as the target object, explore product Mo - TiO2 photocatalytic performance. The main content of this paper to explore and experiment The fruit is as follows: By steam distillation water soluble agent, [CH3(CH2)3O]4Ti as precursors, and （NH4)6MoO24·H2O as Mo source, using sol-gel method Mo - TiO2 photocatalyst, explore different Mo doping quantity, calcining temperature, calcining time on the TiO2 structure, morphology and light push performance, the influence of Mo - results show that the product structure of TiO2 are anatase type, changed and Mo doped TiO2 crystal phase temperature; Aiming at methyl orange degradation, experiments to explore the differen