煤焦油沥青纤维的不熔化过程研究.pdfVIP

999 5 CARBON TECHNI UES 999 l 5 Q 03 SUM 03 刘春林, 吕春祥, 凌立成, 刘朗 ( 中国科学院 山西煤炭化学研究所, 山西太原030001) : (255 e ) , , ( GA) DTATG , : ; 340 e , 200~ 340 e : ; ; :T Q536. 2 :A : 1001-3741( 1999) 05-0001-04 STUDY ON THE STABILIZATION PROCESSES OF COAL TAR PITCH FIBERS L IU Chu -li , LU Chu -xia g, LING L-i che g, LIU La g ( I stitute of Coal Chemist ry, Chi ese Academy of Scie ces, T ia yua 030001, Chi a) Abstract: High soft e i g poi t ( 255 e ) coal t ar pitch w as prepared by t he aid of sulfur. Usi g these coal tar pit ch as st art i g mat erials, carbo f ibers w ere obtai ed by melt spi i g, oxidat ive st abilizatio a d carbo izat io . The stabilizat io processes of as-spu fibers w ere studied by IR, TG/ DTA, GC, eleme tal a alysis etc., a d t he ef fect of fi al oxidat ive st abilizatio temperat ure o t he te sile st re gth of result a t carbo f ibers w as i vest igated. The re- sults show that the fi al stabilizat io tem erat ure has stro i flue ce o the tesile stre t h of carbo fibers, a d o p g g clear w ei ht ai a d exot herm ic he ome o are observed, a d the oxidatio reactio of coal t ar itch fibers w ith g g p p ox e mai l takes lace betwee 200 to 340 e duri the stabilizatio rocess. yg y p g p Ke words: Coal-t ar itch ; carbo f iber ; st abilizat io y p , , [1~5],