放电等离子烧结中颗粒颈部长大“自调节”机制的研究.pdfVIP

放电等离子烧结中颗粒颈部长大“自调节机制的研究 刘雪梅，宋晓艳木，张久兴 北京工业大学材料学院／新型功能材料教育部重点实验室，北京100124 摘要本文以纯铜球形粉末颗粒为烧结原料，研究放电等离子烧结(SPS)过程中颈部组织的演变特 征，并建立模型进行定量描述。对同一颗粒与周围多个颗粒接触表面形成的各颈部的温度分布进行 计算，结果表明，在某一烧结温度下尺寸小的颈部由于温升高于尺寸大的颈部而发生优先长大，随 烧结过程的进行颗粒间颈部尺寸分布趋于均匀化。据此，我们提出SPS过程中粉末颗粒烧结颈部组 织的演变具有独特的“自调节”特征。模型预测结果得到了实验结果的证实。 关键词SPS；颈部长大；温度分布；“自调节”机制 中图分类号：TFl24 onmechanismof neck ofconductivematerials Study homogeneousgrowth pure SPS during Liu Xuemei，SongXiaoyan,ZhangJiuxing ofMaterialsScienceand ofAdvancedFunctional College Engineering，KeyLaboratory Materials，China MinistryofEducation,BeijingUniversity 100124．PChina ofTechnology,Bering neck of Abstract：Inthis mechanismof conductivematerials paper,the homogeneousgrowth pure during SPSis the asthe characteristicsof material，microstructure studied．Byusingpurecopperpowderssintering different arestudied．Itisfoundthattheneckisincreasedwhenthe is stages sintering sintering temperature andtheneckdistributionis atthesame is model increasing homogeneoussinteringstage．Amulti—particle todescribethe distributionofdifferentnecksformedatthesame is developed temperature particle．It from oflesssizeneck concludedthe model is thanthe present