应用低场核磁共振技术测定茶叶含水量.pdfVIP

茶 叶 科 学 2010 ，30 （6 ）：440~444 Journal of Tea Science 应用低场核磁共振技术测定茶叶含水量 1 1 1 1 1,2 1,2* 李然 ，陈珊珊 ，俞捷 ，杨磊 ，汪红志 ，张学龙 （1. 上海理工大学医疗器械与食品学院，上海 200093 ；2. 上海医疗器械高等专科学校，上海 200093 ） 摘要：本研究应用一种更为快速、准确、无损的低场核磁共振技术来测定茶叶的含水量。实验通过标定 6 种不 同质量的纯水标样的 FID 信号幅值，拟合出水分含量与 FID 信号幅值的直线方程，再选取 5 个茶叶样分别测 量其 FID 信号幅值，根据拟合直线换算成茶叶含水量，同时将核磁共振法测得的含水量结果与国家标准的 103 ℃恒重法比较分析。实验结果表明：应用低场核磁共振测定茶叶含水量方便迅速，结果稳定准确，通过与国家 标准的茶叶含水量 103℃恒重法对比发现，核磁共振法测得的含水量偏高不到 1%，这是由于烘干法无法将茶 叶内部的结合水完全烘干所致，而核磁共振法测量的是茶叶内部游离水和结合水的总和。 关键词：茶叶；含水量；低场核磁共振；FID 中图分类号：TS272 ；O661.1 文献标识码：A 文章编号：1000-369X（2010 ）06-440-05 Determination of Water Content of Tea by Low Field Nuclear Magnetic Resonance Technology 1 1 1 1 LI Ran , CHEN Shan-shan , YU Jie , YANG Lei , WANG Hong-zhi 1,2, ZHANG Xue-long1,2* (1. College of Medical Instrument and Food Sciences, University of Shanghai for Scinece and Technology, Shanghai 200093, China; 2. Shanghai Medical Instrumentation College, Shanghai 200093, China) Abstract: Research on the determination of water content of tea by using low field NMR instrument has been conducted. The purpose is to develop a more rapid, accurate and nondestructive method to measure the water content of tea. In this experiment, six pure water samples with different weights were prepared as standard samples to test their FID signals. FID signal data were fitted to a line equation. Five tea samples were prepared to test their FID signals and calculate the water content of tea by the fitting equation, then compare the results with national standard method. Result