Effective Surface Exfoliation of 4H-SiC Induced by He+ and O+ Coimplantation.pdfVIP

Effective Surface Exfoliation of 4H-SiC Induced by He+ and O+ Coimplantation.pdf

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Effective Surface Exfoliation of 4H-SiC Induced by He+ and O+ Coimplantation.pdf

2009 IMP HIRFLAnnualReport 97 References [1]R.A.Hakoort,A.vanVeen,P.E.Mijnarends,AppliedSurfaceScience,85 1995 271 [2]R.S.Brusa,G.P.Karwasz,N.Tiengo,Phys.Rev.。B61 2000 10 154. E3]A.vanVeen,H.Schut,P.E.Mijnarends,In:P.Coleman Ed. ,PositronBeamsandTheirApplications.WorldScien tific,2000 Chapter6 . 3—14 EffectiveSurfaceExfoliation of4H-SiC Inducedby He+ andO+Coimplantation LiBingsheng,ZhangChonghong,ZhangIiqingandZhouLihong 4H—SiC waferswereimplantedwithHe andO ionsseparatelyorcooperativelyatthetemperatures of340 ℃ and380 ℃ ,respectively.AfterHeionimplantation,thesampleswereannealed invacuum ≤ 10一 Pa at800 ℃ for1h,asshown inTable1.Surfacemorphologiesofas—implantedand samplesan— nealedat1000 ℃ for2hwerestudiedbyscanningelectronmicroscopy JSM一6701FSEM .Astoas—im— plantedsamples,therearealotofsymmetricaldistributedcratersand blistersonthe surface shown in Fig.1 SEM imagesoftheas—implantedsamples,a A1,b A2,c A3,andd A4. Fig.2 SEM imagesofthesamples,a A1.b A2,c A3, Fig.3 A crosssectionalSEM image ofa blister in the andd A4annealedat1000 ℃ for2hinArambient. sampleA1annealedat1000℃ for2hinArambient. Fig.1.On thesurfaceofthesampleA 1,thediameterofacratercanreachover6 “m ,asshowninFig. 1a .W econsiderthattheoriginofthecarterresultsfrom thecoalescenceofimplant—induced blistersand over-Dressuredblistersburstinto thepopped—offstateL’ .Thedepthofcraterscan reach about210nm observedbyatomicforcem icroscopy notshown ,whichiswellconsistentwith thedepthofthedamage peak producedby He-implantation.W hen thesampleisimplantedwith Heionsto adoseof3.5× 1O cm_。,ithassim ilarmorphologyasA 1thattherearealotofcraterssurroundedbyblisters.However,the densityofcratersofA2issmallerthan thatofA1.M eanwhile,themeanmagnitudeofblistersofA2is smallerthan thatofA1.Astoannealedsamples,itwasshownthattheselecteddos

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