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Microchemical Journal 121 (2015) 107–111
Contents lists available at ScienceDirect
Microchemical Journal
journal homepage: /locate/microc
A reagentless flow injection system for the quantification of ethanol in
beverages based on the schlieren effect measurement
Susana S.M.P. Vidigal, António O.S.S. Rangel ⁎
CBQF—Centro de Biotecnologia e Química Fina, Laboratório Associado, Escola Superior de Biotecnologia, Universidade Católica Portuguesa/Porto, Rua Arquiteto Lobão Vital, Apartado 2511,
4202-401 Porto, Portugal
a r t i c l e i n f o a b s t r a c t
Article history: A flow injection system comprising a gas-diffusion unit and schlieren effect detection was arranged in order to
Received 19 January 2015 develop a simple methodology for the quantification of ethanol in different alcoholic beverages. It was possible
Received in revised form 19 February 2015 to establish a linear range up to 25% (v/v), with a LOD and a LOQ of 0.6% and 2.0% (v/v ), respectively; with
Accepted 22 February 2015
good repeatability, RSD b 4.6%. Only 80 μL of sample was needed for quantification with a determination rate
Available online 28 February 2015
of one determination per minute.
Keywords: To evaluate the accuracy of the proposed method, a total of 43 alcoholic beverages, red and white table wine, port
Flow-injection system wine, beers, liquors, spirits and brandies were analysed. The results obtained by the develo
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