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半芳香共聚尼龙6T_6的合成与表征_张春祥.pdf
41 10 Vol.41No.10 13 2013 10 ENGINEERING PLASTICS APPLICATION Oct. 2013
doi:10.3969/j.issn.1001-3539.2013.10.003 6T6 * 12 1 13 2 12 1 1. 211167 2. 215617 3. 210094 PA 6T PA6T 6 PA6T 190 3 h TQ323.6 A 1001-3539 2013 10-0013-04 Preparation and Characterization of Semi-Aromatic Co-Polyamide 6T6 1 2 1 1 3 2 1 2 1 Zhang Chunxiang Feng Zhiming Zhang Shengchun Gu Xiaohua Han Bing Zhang Kejie 1. School of Materials and Engineering Nanjing Institute of Technology Nanjing 211167 China 2. Research Center on Engineering Technology of Industrial Chemical Fibers Zhangjiagang 215617 China 3. School of Chemical Engineering Nanjing University of Science and Technology Nanjing 210094 China Abstract: Serious of semi-aromatic copolyamides 6T6 were synthesized via solution polymerization by using hexamethy-
lenediamine salt of terephthalic acid PA6T salt and caprolactam as raw materials. The structure of obtained samples were
characterized by fourier transform infrared spectroscopy and differential scanning calorimetry. The in? uence of co-monomer ratio
polymerization temperaturepolymerization time and other process factors on the melting pointintrinsic viscosity was discussed in
detail. The results show that with increasing the amount of substance ratio of PA6T saltcaprolactamthe melting points of PA6T
6 show an increasing trend after the ? rst reduction. The increase in the solid-phase reaction temperature and time is conductive to the
increase of intrinsic viscosity. The optimum polymerization conditions are 190 for 3 h. The effect of solid-phase polymerization to
raise the melting point of co-polyamide is not obvious. Keywords: semi-aromatic co-polyamide solid phase polymerization characterization PA6T 30% [12] PA1212 PA12T PA121212T [1–6] PA [14] PA PA PEEK * BK座机电话号码 11KJB430008 YKJ201202YKJ201209 [7–14]T. F. Novitsky [8] PA10TPA12T PA6T 2013-08-02 14 2013 41 10 PA6T KBr 4004 000 cm1
PA6T6 DSC PA6T6 10 min 2
1 21
11 PA6T 1 1 PA6T pH 7
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