Fe粉在介质阻挡放电辅助高能球磨中行为研究.pdfVIP

C23 Fe 粉在介质阻挡放电辅助高能球磨中的行为研究 1 1 1 2 戴乐阳 ，林少芬 ，陈清林 ，杨小平 （1. 集美大学轮机工程学院 福建厦门 361021 2. 华南理工大学材料科学与工程学院 广东广州 510640 ） 摘要：利用介质阻挡放电辅助高能球磨方法对 Fe 粉进行球磨，10h 后即可获得平均粒径 100nm 左右的纳米 Fe 粉。通过扫描电镜、透射电镜和 BET 比表面积测试，观察Fe 粉在不同球磨时间后的表现行为，分析球磨中介 质阻挡放电的协同作用机制。扫描电镜结果表明，在介质阻挡放电的作用下，辅助球磨初期的 Fe 粉显示出极 优越的塑性性能，其变形程度远大于普通球磨。而从辅助球磨 10h Fe 粉的透射电镜观察可见，由于介质阻挡放 电的电子冲击对Fe 粉诱发热爆效应，球磨时能大量形成粒径 50nm 左右的 Fe 粉颗粒。研究表明，辅助球磨中 介质阻挡放电所带来的热效应和热爆效应，能有效促进 Fe 粉的球磨细化进程。 关键词：介质阻挡放电；高能球磨；纳米 Fe 粉；电子冲击；热爆 Investigation on the behavior of Fe powder during high-energy ball milling assisted by dielectric barrier discharge 1 1 1 2 DAI Leyang , LIN Shaofen , CHEN Qinglin , YANG Xiaoping (1. Marine Engineering Institute, Jimei University, Xiamen 361021, China; 2. School of Material Science and Engineering, South China University of Technology, Guangzhou 510640, China) Abstract: Nano-Fe powders could be prepared only after 10 hours of high-energy ball milling assisted by dielectric barrier discharge (DBD), whose particle mean size was about 100nm. The synergism mechanism of DBD on ball milling has been investigated by examining the behavior of Fe powder using scanning electron microscopy, transmission electron microscope and BET method. It was shown through SEM that Fe particles displayed an extraordinary plasticity in the early assisted milling stages under the action of DBD, and the plastic deformation of Fe particles was more severe than in normal milling. Large quantity of Fe particles about 50nm were observed by TEM which were generated during ball milling owing to the hot explosion effect of