Fe-Cr非晶的制备和热稳定性初步研究.pdfVIP

The 6th China Corrosion Conference   Fabrication and Thermal Stability of Amorphous Fe-Cr Alloy Coating: Preliminary Investigation 1 2 2 2 Zhuqing CHENG , Yunhan LING , Song WANG , Xinde BAI 1Department of Engineering Physics, Tsinghua University, Beijing, China, 100084 2Department of Materials Science and Engineering, Tsinghua University, Beijing, China, 100084 Email: czhq07@163.com, yhling@ Abstract: Amorphous Fe-Cr alloy coating was fabricated by bidirectional pulsed electrodeposition process, and the surface morphology and microstructure of the coating were examined by scanning electron micros- copy (SEM), X-ray diffraction (XRD) and transmission electron microscopy (TEM), respectively. The stabil- ity of the as-deposited coating was investigated via vacuum annealing and hydrothermal soaking. The pre- liminarily experimental results indicated that the electrochemical corrosion resistance and thermal stability of the coating decreased obviously after annealing and hydrothermal treatment. Keywords: Amorphous iron-chromium alloy; bidirectional pulsed electrodeposition; vacuum annealing; hydrothermal treatment; thermal stability Fe-Cr 非晶的制备与热稳定性初步研究 1 2 2 2 程竹青 ，凌云汉 ，王松 ，白新德 1 清华大学工程物理系，北京，中国，100084 2 清华大学材料科学与工程系，北京，中国，100084 Email: czhq07@163.com, yhling@ 摘 要：使用双向脉冲电沉积法制备了Fe-Cr 非晶镀层，用扫描电镜（SEM ）、X 射线衍射（XRD ）和 透射电镜（TEM ）研究了镀层的表面形貌和组织结构。对Fe-Cr 非晶镀层进行真空退火处理和高压釜 水热处理，利用SEM 和XRD 研究了处理后镀层的变化，并用电化学工作站测量了极化曲线，结果表