高效液相色谱法测定细胞裂解液中多胺含量_刘小琴.pdfVIP

2010 30 13 Chin H osp Pharm J , 2010 Jul, Vol 30, No. 13 # 1159 # - 1 0 . 0 07 2 g#L 1 mL0 , , , 2. 5. 3 1 mL ( RSD 0 . 3 6% , n = 5) ( RSD , 4 mL, , 80 % , 1. 7 1% , 0, 2, 4, 6, 8, 10, 12 h ) ( RSD 0 . 51% , -1 3 00 0 r#m in 2 0 min, , 50 mL n= 5) , 10 1. 93 % , RSD 1. 62% ( n= 5) , , , 2 mL, 3 , , / 4 % 2, 3 2 Tab 2 Results of ort