射干X射线衍射Fourier指纹图谱鉴定.pdfVIP

ANDMATERIA I,ISH职HENMEDICINE MEDICARESEARCH2010VOL．21NO．I 时珍国医国药2010年第21卷第l期 ◇国药鉴别◇ 射干的X射线衍射Fourier指纹图谱鉴定 杨红玲，吴呜建+，沈国鹏 (郑州大学化学工程学院，河南郑州450001) 摘要：目的建立射干药材XRD的鉴定分析新方法。方法采用粉末x射线衍射Fourier指纹图谱鉴定法。结果通过对 5个射干中药材进行实验、计算分析，获得了各样品的Fourier指纹图谱、特征标记峰值和相似度，并结合x射线衍射半定 量相分析比较各个组分中仪一石英、一水草酸钙、蔗糖的含量。结论X射线衍射Fourier指纹图谱鉴定法可用于中药材 射千的鉴定。 关键词：射干； 药材鉴定；XRD指纹图谱；半定量；相似度 中图分类号：R282．5文献标识码：A 文章编号：1008旬805(2010)01-0181-02 onRhizomaBelamcandaediffractionFourier PrintPat- Identification byX—ray Finger tern Method YANG Hong—ling，WUMing-jian’，SHENGuo—peng Chemical 450001，China) (Collegeof Engineering，ZhengzhouUniversity，Zhengzhou To aHewidentificationand methodofRhizomaBelamcandae．MethodsPowder Abstract：Objective X—ray develop analysis diffraction was and carriedoutonfive diffraction Fourier used．Results were pattern Experimentsanalysis samples．TheX—ray Fourier andcharacteristicdiffractionofRhizomaBelamcandaewere was finger pattern peaks obtained，andQXRDanalysis print usedto theconterts oxalate inall Thismethodcallbe compare of仅一quartz、calciummonohydrate，sucrosecampses．Conclusion usedforidentificationofChinesemedicinalmateriasofRhizomaBelanwamtae． Fourier IdentificationonChinesemedicinal diffraction Keywords：RhizomaBelamcandae； materias；X—ray pattern； Similar QXRD； degree 射干是鸢尾科射干属植物射干Belamcandachinensis(L．)射法与粉末X衍射法。物质组成、晶型、分子内成键方式、分子 DC的干燥根茎，为常用中药，已被收载于《中