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Materials Chemistry and Physics 128 (2011) 303–310 Contents lists available at ScienceDirect Materials Chemistry and Physics j o u rn al h omepage: w w w. elsev /locate/matc hemphys Study of Ni-catalyst for electroless Ni–P deposition on glass fiber Libo Li ∗ , Bo Liu School of Chemical and Environmental Engineering, Harbin University of Science and Technology, No. 4 Lin Yuan Road, Harbin 150040, People’s Republic of China a r t i c l e i n f o a b s t r a c t Article history: The glass fiber surface is metalized with electroless nickel–phosphorus deposition. The roughening and Received 1 August 2010 activation processes are optimized by the orthogonal experiments. A new nickel-catalyst method is devel- Received in revised form 26 January 2011 oped to activate the glass fiber surface. When the activation is completed, a layer of continuous and dense Accepted 14 March 2011 film is formed on the substrate. The activated film contains a great deal of nickel oxide particles which can become the active sites after they are deoxidized in the electroless bath. In the activated film on Keywords: the glass fiber, the content of Ni element is 41.01 wt.%, the content of O element is 45.64 wt.% and the Glass fiber surfaces content of P element is 13.35 wt.%. Scanning electron microscopy (SEM) shows that the Ni–P coatings Electroless nickel–phosphorus alloy coatings