总氮测定中过硫酸钾的影响.pdfVIP

23 4 V ol. 23, N o. 4 2 0 1 0 8 POLLUT ION CONTRO L TE CHNOLOGY A ug ., 2 0 1 0 监测技术 1 2 1 1 , , , ( 1. 湖南农业大学资源环境学院, 湖南 长沙 410128; 2. 西南有色昆明勘测设计院股份有限公司, 云南 昆明 65005 1 : - !( GB 11894∀ 1989 , , K S O , 2 2 8 : , , , , : ; K S O ; 2 2 8 : X 832; X8305 : A The E ffects of P otassium P ersu lfate on T otal N itrogen D eterm ination 1 2 1 1 ZHOU X ish i, Q IN Y ingfeng , L IU L i, L I X ihong ( 1. College of Resources and Environment, H unanAgricultural University, Changsha, H unan 410 128, China; 2. Southw estN onf errous unm ing Survey and D esign Institute, unm ing, Yunnan 650051, China) A bstrac t: The accuracy o f tota l n itrog en dete rm ina tion in w a ter fo llow ing GB 11894 - 19 89 w as o ften affected by h igh blank va l ue. T his study discu ssed the mi pacts on the blank va lue, the standard curve and the smi ulated w ate r sam ples through the repea ted recrystalliza tion processing o f potassium persu lfate. T he resu lts show ed that the recrysta lliza tion o f potassium persu lfate cou ld reduce the b lank va lue in de term ination o f tota l n itrog en effec tive ly, mi prove the sens itiv ity o f the standard curve, expand the determ ination rang e and mi prove the accu racy of the determ ination results. K ey w ord s: tota l n itrog en; potass ium pe r su lfate; influenc ing fac to r , 1 1. 1 器