超临界CO_2萃取工艺对蛇床子提取物提取率的影响_宫竹云.pdfVIP

2006 8 中成 药 Augu st 2006 28　 8 Chine se T raditiona l P atentM ed icine V o l. 28　N o. 8 [　　] CO2 * 宫竹云, 　张高勇 , 　聂永亮, 　谷惠先 (中国日用化学工业研究院, 山西太原 030001) :;;; :: CO2 。:, (ⅠⅡ)。:: 20 M Pa, 40 °C;Ⅰ 15 M Pa, Ⅰ 65 °C;Ⅱ 5M Pa, Ⅱ 38 °C;CO 18 L H, 80 m in。: 2 , 24. 03 。 。 :R 284. 1　　　　　:A 　　　　　:1001-1528(2006)08-1102-06 Influence of the technology of supercriticalCO extraction on the separate 2 rate of the extractives from fruits ofCn idium M onn ieri (L. )Cuss. * GONG Zhu-yun, 　ZHANG Gao-yong , 　N IE Y ong-liang, 　GU H u-i xian (Ch ina R esearch In st itu te of D a ily Chem ica l Industry, Ta iy uan 030001, Ch ina ) KEYWORDS:supe rcritical;the extrac tives from fruits of Cn id ium M onn ieri(L. )Cu ss;extrac tive ra te;seconda- ry reg ression cohe rent design BSTR CT: IM:To u se secondary regression coheren t design to explo re the extraction param e ters of fruits o f Cn id iunm by supercritical CO2 extraction. METHODS:Ex traction pressure, extraction tem pe ra tu re, iso lation pressu re, iso lation tem pe ratu re Ⅰ and Ⅱ we re v iewed as factors. RESULTS:T he best technolog ical conditions w ere:ex tractive ke ttle pressu re was 20 MP a, ex tractive ke ttle tem perature w as at 40 °C;sepa ra te ke ttle Ⅰ p ressure w as 15 MP a, separate kettle Ⅰ tem perature w as at 65 °C;separate ke ttle Ⅱ pressure w as 5 M Pa, separate ketle Ⅱ temperature w as a t 38 °C;CO2 flow rate was 18 L H, ex tractive tmi e w as 80 m in. CONCLUSION:Under these conditions, the separate ra te o f the ex tractives from fru its o fCn id ium M onn ieri(L. )Cu ss. could be 24. 0 3 . U sin