啤酒中甲醛含量国标测定方法的研究.pdf

# 352# 2009 12 8 6 Ch in ese Jou nal of Pub licH ealth E nginee ing Dec1 2009, V ol1 8 No16 = 刘跃坤 (吉林市疾病预防控制中心, 吉林 吉林 13200 1) = , RSD 11 8% ~ 312% , 96% ~ 103% , , r = 01999 7 , , = ; ; 12 R155; O65713 12 A 12 1671-4199( 2009) 06-0352-03 Determ inationM ethod for Form aldeh de in Beer of National Standards LI U Yue - kun1J ilin M un icpi al Centerf or D isease Con tro l and P reven tion, J ilin J ilin 132001, Ch ina = Abstract Objective T o establish a new me thod fo dete m ination of fo m a ldehyde in bee based on national stand- a ds1M ethods K jeldahl distillation un it and vacuum distillation un its eplaced steam unit fo ex t ac ted f om the fo m alde- hyde in bee based on the national standa ds, and mi p oved thew ate bath tem pe a tu e1R esults The elative standa d de- v iation of the new m ethod was 11 8% - 31 2% , the ecove y ate was 96% - 103% w ith a good linea ang e, co e lation co- efficient w as 01 999 71Conclusion T hism e thod has the cha acte istic of good p ec is ion and high accu acy fo the de te m -i nation of fo m a ldehyde in bee 1 = Ke words Bee ; F o m a ldehy; De te m ination m ethod , 1 000 m l, , WHO 90 m l() , , 100 m l 11, 22 GB /T 11213 10 m l 25 m l 132 5009149- 2003 , , 2 m l , 60e 30 m in, , , ( 0015110210310510 Lg; 1 01006 701017 201028 301052 201073 6 111 ( 01120 6, r = 01999 9) , 1 cm ); 4 14 nm ( 1B1); , 014 m l