聚对苯二甲酸乙二酯轧制及加热过程中的织构研究.pdfVIP

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聚对苯二甲酸乙二酯轧制及加热过程中的织构研究.pdf

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第23 卷第5期总第97 期 Vol 2 3 No 5 Journal of Materials Science Engineering Oct . 200 5 :1004793X 2005 0座机电话号码 2 3 , ,D. Raabe , 1. , 100083;2.MaxPlanckInstitut fr Eisenforschung, MaxPlanckStr. 1, D40237, Dsseldorf, Germany;3. Engineering Division, Colorado School of Mines, Golden, CO80401, USA X PET , PET , 00 , , ; PET , , X PET , , , PET 00 [00 ] ; ; X : O63 . :A Investigation of Crystallograp ic Texture in Rolled and Heat Treated of Polyet ylene Terep t alate 1 1 2 3 CHEN Leng , MAO Weimin , RAABE D , CHEN Nan 1. Department of Materials, University of Science and Tec nology Beijing, Beijing 100083, C ina; 2. MaxPlanckInstitut fr Eisenforsc ung, MaxPlanckStr. 1, D40237, Dsseldorf, Germany; 3. Engineering Division, Colorado Sc ool of Mines, Golden, CO80401, USA Abstract The crystallographic texture of semi crystalline PET was investigated during cold rolling and heat treatment based on the Xray diffractometer equipped with an area detector . Experimental result indicates that the rolling texture consists of a 00 component and an incomplete fiber rolling direction . Both texture components were enhanced and the textures developed at high temperature faster than low temperature during subsequently heat treatment. The crystallinity of PET in heat treatment process was calculated using the average Xray diffraction intensity collected by an area detector . The result of calculation reveals that crystallinity decreases drastically during cold rolling and increases gradually during heat treatment. It is considered that the 00 component induced by cold rolling could be explained by the mechanism of 00 [00 ] molecule chain glide. Key words PET ; texture; Xray diffraction PET [ 4] 1 前言 ,Mahendrasingam [5] PET , Bedia PET PET , , PET PET , , PET [ ] [ 2] , , , [ 3] , , PET , , , , :2004 9; :20050 24 : 964- , , , . ? 474 ? 2005 0 , PET , , 00 , , 3.2 PET PET , PET . 2 PET 00!C 200!C , , 00 0 0 0 2 3 X PET 00 0 0 0 , , X , PET