半夹心铱、铑的氮碳硼烷和双齿卡宾化合物的合成及结构研究.pdfVIP

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半夹心铱、铑的氮碳硼烷和双齿卡宾化合物的合成及结构研究.pdf

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半夹心铱、铑的氮碳硼烷和双齿卡宾化合物的合成及结构研究

目录中文摘要 ··················································································…… I 英文摘要 ··················································································…… H 第一章前言 ················································································… … 1 1.1 碳硼烷及其金属化合物 ·····························································…… 1 1.2 双齿氮杂环卡宾及其金属化合物 ·················································……7 1.3 选题依据 ·············································································… … 11 1.4 参考文献 ···············································································一 H 第二章含双氮杂环卡宾配体的半夹心铱、锗、钉金属有机化合物 ············……19 2.1 前言 ··~ ···············································································… … 19 2.2 结果与讨论 ··········································································… …2 0 2.2 .1 配体 l一sH 一2一(洲一)e 伽 H R )e ZB ，oH lo(R 一P‘r(l)，e y (2))的合成及结构表 …20 2.2 .1 化合物 (e p *M ) [l一sH 一2一(R N 一)C 州 H R )C ZB loH lo] (M Ir(a)，R h (b)，R ，pr(l)， C y (2 )) 的合成及结构表征 ·············································… … 2 1 2.3 实验部分 ························，····················································… …2 8 2.3.1 原料及试剂 ·····································································… …2 8 2.3 .2 分析及测试 ·····································································… …2 8 2.3.3 化合物的合成步骤及结构表征 ·············································……2 8 2.4 本章小结 ·······································································…… ”””31 2 .5 参考文献 ·············································································… …31 第三章含双氮杂环卡宾配体的半夹心铱、铭、钉金属有机化合物 ············……34 3.1 前台- ···················································································… …3 4 3.2 结果与讨论 ··