《Unexpected luminescence enhancement of upconverting nanocrystals by cation exchange with well retained small particle size》.pdfVIP

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《Unexpected luminescence enhancement of upconverting nanocrystals by cation exchange with well retained small particle size》.pdf

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《Unexpected luminescence enhancement of upconverting nanocrystals by cation exchange with well retained small particle size》.pdf

DOI10．1007／s12274．01 Res∞rchArticle Unexpectedluminescenceenhancementofupconverting nanocrystalsbycationexchangewithwellretainedsmall particlesize MingliangDengandLeyuWang(囟 ) StateKeyLaboratoryofChemicalResourceEngineering,BeijingKeyLaboratoryofEnvironmentallyHarmfulChemicalAnalysis, SchoolofScience,BejiingUniversityofChemicalTechnology,Bejiing100029,China Received：16January2014 ABSTRACT Revised：28February 2014 Highlyluminescentupconversionnanoparticles(UCNPs1withsmallsizesare Accepted：02M arch2014 highlydesirableforbioapplications．A facileinsitucationexchangestrategyhas been developed to greatly enhance theUC luminescenceofhexagonalphase ◎TsinghuaUniversityPress NaYF4NPswhilemaintaining theirsmal1particlesizeandshape．Viaacation and Springer-Verlag Berlin exchangetreatmentbyhot—injectingGd precursorsintotheas—preparedNPs Heidelberg2014 solutionwithoutpre--separation,thenaked．．eyevisibleUC emissionoftheNPs wasehn ancedabout29timesunder980nrnnearinfraredfNIR1excitationwith KEYWoRDS unchangedparticlesize．Thecationexchangeprocesswasfurtherdemonstrated cationreplacement, forthecaseofNaYF4nanorods(NRs)．Afterhtecationexchange，htenanorodwas upconversion brokenintotwoNPswiht strongeremission．Th ecationexchangedhydrophobic lum inescence， UCNPswerefurtherencapSulatedwihtpoly(aminoacid、andsuccessufllyapplied cellimaging, fortargetedcancercellUClum inescenceim aging． luminescenceenhancement 1 Introduction near—infrared (NIR)irradiation，high photostability, goodhcemicalstability,andlowcytotoxiciyt,rare—-earth—- Asbiomarkers,luminescentnanoparticles(NPs)should dopedupconversion(UC)luminescencen