五子补肾胶囊的制备工艺及质量控制方法研析.pdf

目 录 中文摘要··················································································1 英文摘要··················································································3 引 言··················································································6 正 文··················································································7 第一部分 五子补肾胶囊提取工艺研究···········································7 1 实验材料···············································································7 1.1 实验用对照品及药材····························································7 1.2 实验主要仪器及试剂····························································7 2 实验方法···············································································8 2.1 处方研究与分析··································································8 2.1.1 处方组成 ········································································8 2.1.2 提取工艺分析 ··································································8 2.1.3 考察指标的选择·······························································9 3 五子补肾胶囊水提部分正交试验··············································10 3.1 实验方法·········································································10 3.1.1 水提取工艺正交试验设计·················································10 3.1.2 煎煮试验样品的制备·······················································10 3.1.3 含量测定方法 ································································10 3.2样品的测定·······································································12 3.3 得膏率的测定 ···································································13 3.4 实验结果·········································································14 3.4.1 正交试验水平设计表及结果··············································14 3.4.2 正交实验结果方差分析····················································15 3.5 水提取工艺正交实验结果验证性实验·····································15 3.6 小结·········································