血液中酒精含量的測定外文文献.docVIP

1. Microdetermination of alcohol in blood by gas-liquid chromatography. 气液色谱法测定血液中的微量酒精 Computer-aided headspace gas chromatography applied to blood-alcohol analysis: importance of online process control.计算机辅助顶空气相色谱法测定血液中的酒精：在线过程控制的重要性。 This paper describes the analysis of ethanol in blood specimens（标本） from suspect drunk drivers and the associated quality assurance procedures currently used in Sweden for legal purposes.（目前在瑞典使用的以法律为目的的相关质量保证程序） Aliquots（等分试样） of whole blood from two separate Vacutainer tubes（真空采血管） are diluted（稀释） with 1-propanol （丙醇）as internal standard before analysis by headspace gas chromatography (HS-GC) with three different stationary phases: Carbopak B, Carbopak C, and 15% Carbowax 20 M（聚乙二醇）. The actual HS-GC analysis, the integration （整合）of chromatographic peaks, the collection and processing of results, as well as the quality control tests involve the use of computer-aided techniques. The standard deviation （误差，偏差）of analysis(y) increased with concentration of ethanol in the blood specimen(x), and above 0.50 mg/g the regression equation （回归方程）was y = 0.0033 + 0.0153x. The prosecution（起诉） blood-alcohol concentration (BAC) is the mean of three separate determinations made by different laboratory technicians working independently with different sets of equipment. A deduction（推论） is made from the mean analytical result to compensate（补偿） for random and systematic errors inherent in the method. At BACs of 0.5 and 1.5 mg/g, which are the statutory（法定的） limits in Sweden, the allowances currently made are 0.06 and 0.09 mg/g, respectively. Accordingly, the reduced prosecution BAC is less than the actual BAC with a statistical confidence of 99.9%. 4.Direct blood-injection method for gas chromatographic determination of alcohols and other volatile compounds（挥发性化合物）.5. Variability of the blood/breath alcohol ratio in drinking drivers.The ratio of blood-alcohol concentration (BAC) to breath-alcohol concentration (BrAC) was determined for 799 indiv