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MUDMASTER: A PROGRAM FOR CALCULATING CRYSTALLITE SIZE DISTRIBUTIONS AND STRAIN FROM THE SHAPES OF X-RAY DIFFRACTION PEAKS By D. D. Eberl1, V. A. Drits2, J. írodo~3 and R. Nüesch4 1U.S. Geological Survey, 3215 Marine St., Boulder, CO 80303-1066 USA; 2Institute of Geology RAN. Pyzevskij 7, 109017 Moscow, Russia; 3Institute of Geological Sciences PAN, Senacka 1, 31002 Krakow, Poland; 4ETH, Zurich 8092, Switzerland. _________________________________________________________ U.S. Geological Survey Open-File Report 96-171 __________________________________________________________ Boulder, Colorado 1996 U.S. DEPARTMENT OF THE INTERIOR BRUCE BABBITT, Secretary U.S. GEOLOGICAL SURVEY Gordon Eaton, Director Last revised: August 16, 2000 Cover SEM photo of dickite crystals from the San Juan Mountains (Colorado) by Howard May. For additional information and a copy of the program, write or e-mail: Dennis D. Eberl U.S. Geological Survey 3215 Marine Street Boulder, Colorado 80303-1066 USA ddeberl@ CONTENTS Page “Mud Master” by Wallace Stevens 5 Introduction 6 System Requirements and Disclaimer 8 Structure of MudMaster 8 Installation of MudMaster 9 Data Required 10 Examples 11 Example 1: A Simple Analysis 11 Example 2: Using PeakPicker and Doing the Flip 17 Example 3: Symmetrical Strain Analysis 22 Other Examples: MOM, HUMPS, MUM, Mt. Washington, and ZEMP-PVP 25 Standards 26 Other Analytical Hints 27 Acknowledgments 28 References 28 Appendix 1: Summary of Program Inputs 30 Table 1. Summary of PeakPicker (pp.xls) Inputs 30 Table 2. Summary of MudMaster Sheet 1 (1-mm.xls) Inputs 32 Table 3. Summary of MudMaster Sheet 2 (2-mm.xls) Inputs 36 Appendix 2: Recommended Settings for Clay Analyses 37 Table 4. Recommended Settings for Analysis of Clay Basal Reflections 37 Appendix 3: Plots of LpG2 and XRD Patterns for Clay Mineral Basal Reflections 39 Figure 1: Illite 39 Figure 2: 2-Glycol Smectite 40 Figure 3: 2-Water Smectite 40 Figure 4:

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